Product name : cis-5-norbornene-endo-2,3-dicarboxylicanhydride 2hazardsidentification cis-endo-5-norbornene-2,3-dicarboxylic anhydride c9h8o3 164,16g/mol. Safety data sheet methyl-(endo)-5-norbornene-2,3-dicarboxylic anhydride version 2 2/3/2009 - uk 5: fire-fighting measures suitable extinguishing : water spray, dry powder, foam. Diels-alder reaction: preparation of cis-norbornene-5,6-endo-dicarboxylic anhydride(university of colorado, boulder, dept of chem and biochem. Cis-5-norbornene-endo-2,3-dicarboxylic has 100 similiar compounds, including carbic anhydride|cis,endo-5-norbornene-2,3-dicarboxylic acid, providing their melti. Chem 334l organic chemistry laboratory revision 41 a diels-alder synthesis of cis-norbornene-5,6-endo-dicarboxylic anhydride in this laboratory exercise we will synthesize the compound. Were only able to produce a yield of 202% a yield this low was not expected, but was enough to measure the melting point to see if we had indeed produced cis-norbornene-5. Synthesis of cis-norbornene-5,6,-endo-dicarboxylic acid o o o co2h co2h h2o experimental procedure: for preparation of the endo-cis-diacid, place 40 g of anhydride and 50 ml of distilled. I hydrolized the following compound: cis-norbornene-5,6-endo-dicarboxylic anhydride then took the cis-norborene-5,6-endo-dicarboxylic acid and added h2so4 to it (warmed it up and cooled it.
View lab report - diels-alder reaction synthesis of cis-norbornenr-5,6-endo-dicarboxylic anhydride from chm 2211l at university of south florida i introduction diels alder reactions are. Chem 322: diels-alder reaction synthesis of cis-norbornene-2,3-endo-dicarboxylic anhydride introduction in 1921, otto diels and kurt alder discovered that certain alkenes and alkynes can. Cis-endo-5-norbornene-2,3-dicarboxylic anhydride formula : c 9 h 8 o 3 show this safety data sheet to the doctor in attendancemove out of dangerous area. Point properties other cis-norbornene-5,6-endo-dicarboxylic anhydride 16416 0295 g mp 165 oc white plate-like microscale organic experiments. Diels-alder reaction: preparation of cis-norbornene-5,6-endo-dicarboxylic anhydride (university of colorado, boulder, dept of chem and biochem. Cis-norbornene-5,6-endo-dicarboxylic anhydride cyclopentadiene was previously prepared through the cracking of dicyclopentadiene and kept under cold conditions.
Find quality suppliers and manufacturers of cis-5-norbornene-endo-2,3-dicarboxylic endo-norbornene-cis-5,6 5-ene-2endo,3endo-dicarboxylic acid anhydride. A diels-alder synthesis of cis-norbornene-5,6-endo-dicarboxylic anhydride in this laboratory exercise we will synthesize the compound cis-norbornene-5,6-endo.
Sigma-aldrich offers aldrich-247634, cis-5-norbornene-endo-2,3-dicarboxylic anhydride for your research needs find product specific information including cas, msds, protocols and. Cis-5-norbornene-endo-2,3-dicarboxylic anhydride cis-5-norbornene-exo-2,3-dicarboxylic anhydride 1 product result | match criteria: product name. Reaction mechanism the scheme below depicts the concerted mechanism of the diels-alder reaction of cyclopentadiene and maleic anhydride to formcis-norbornene-5,6-endo-dicarboxylic anhydride.
The diels nmr, ir report repaired) repaired) limiting reagent = cis-5-norbornene-endo-2,3-dicarboxylic anhydride theoretical yield of cis-5-norbornene-endo-2,3. Diels-alder reaction: synthesis of cis-norbornene-5, 6-endo-dicarboxylic anhydride introduction: the diels-alder reaction is a [4+2] cycloaddition of a conjugated diene and a dienophile.
In this experiment i used the diels-alder cycloaddition reaction mechanism to form cis - norbornene-5,6-endo -dicarboxylic anhydride from the reaction of the conjugated diene cyclopentadiene. Part i the diels-alder adduct of cyclopentadiene and maleic anhydride, 2-norbornene-5,6-endo-dicarboxylic anhydride, may be rearranged thermally to its exo-isomer. Endo-5-norbornene-2,3-dicarboxylic anhydride endo,cis-5-norbornene-2,3-dicarboxylic anhydride endic anhydride nadic anhydride 3,6-endomethylene-δ4.
Buy high quality carbic anhydride 129-64-6 from toronto research chemicals inc. Essays & papers diels-alder reaction: synthesis of cis-norbornene-5, 6-endo-dicarboxylic anhydride - paper example. Safety data sheet methyl-(endo)-5-norbornene-2,3-dicarboxylic anhydride meth-e revision 11 01/06/2015 - en contains: 1,2,3,6-tetrahydromethyl-3,6-methanophthalic anhydride. Visit chemicalbook to find more cis-5-norbornene-exo-2,3-dicarboxylic anhydride(2746-19-2) information like chemical properties,structure,melting point,boiling point,density,molecular. Although the homopolymer endo-5-norbornene-2,3-dicarboxylic anhydride.
Cis-5-norbornene-endo-2,3-dicarboxylic anhydride is used as an organic chemical synthesis intermediate. Endo-norbornene-cis-5,6-dicarboxylic acid - chemical information, properties, structures, articles, patents and more chemical data. Diels-alder reactions maleic anhydride is a while solid and acts as the with the product being cis-norbornene-5,6-endo-dicarboxylic anhydride. Experiment 2 (organic chemistry ii) pahlavan/cherif diels-alder reaction preparation of endo-norbornene-5, 6-cis-carboxylic anhydride purpose a) study conjugated dienes.